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Title
  • en Electrochemical synthesis of methyl-3,5,7-trifluoroadamantane-1-carboxylate under recycling use of ionic liquid media
Creator
Accessrights open access
Subject
  • Other en Electrochemical fluorination
  • Other en Adamantane
  • Other en Ionic liquid
  • Other en Pyridine-5HF
  • Other en Recycle
  • NDC 431
Description
  • Abstract en Methyl-3,5,7-trifluoroadamantane-1-carboxylate, a key intermediate for the synthesis of 1-amino-3,5,7-trifluoroadamantane (trifluoroamantadine), was synthesized by the electrochemical fluorination of methyl adamantane-1-caroxylate in pyridine-5HF under constant current conditions. After the reaction, the product was extracted from pyridine-5HF by hexane-CH2Cl2, and recovered pyridine-5HF was used repeatedly.
Publisher en Elsevier B.V.
Date
    Issued2012-08
Language
  • eng
Resource Type journal article
Version Type AM
Identifier HDL http://hdl.handle.net/2115/50058
Relation
  • isVersionOf DOI https://doi.org/10.1016/j.jfluchem.2012.04.006
Journal
    • PISSN 0022-1139
      • en Journal of Fluorine Chemistry
      • Volume Number140 Page Start28 Page End30
File
Oaidate 2023-07-26